Effects of Heat Treatment on the Physical Properties and Stress Wave-Based Dynamic Modulus of Elasticity of Camphor Wood (Cinnamomum camphora): A Response Surface Methodology Approach
Abstract
This study investigated the effects of dry-air and hydrothermal heat treatments on the physical properties and stress wave-based dynamic modulus of elasticity (DMOE) of Camphor wood (Cinnamomum camphora) using response surface methodology (RSM). Dry-air treatment was conducted at 150 – 200 °C for 10 – 20 h, whereas hydrothermal treatment was performed at 120 – 150 °C for 60 – 120 min. Equilibrium moisture content (EMC), air-dry density (AD), and stress wave-based DMOE were determined after treatment. Treatment temperature and duration significantly affected the measured properties, although their relative importance varied between the two treatment methods. Increasing treatment severity generally resulted in reductions in EMC, AD, and DMOE. Response surface models adequately described the relationships between the processing variables and the measured responses. Multi-response optimization was subsequently used to identify suitable treatment conditions by considering EMC, AD, and DMOE simultaneously. The optimized conditions differed between the dry-air and hydrothermal processes, reflecting differences in their responses to treatment temperature and duration. The results demonstrate the potential of stress wave-based DMOE as a rapid, non-destructive indicator for characterizing changes in the dynamic stiffness of heat-treated Camphor wood and provide a basis for selecting suitable thermal modification conditions for this species.
References
10.22517/23447214.22641
Ali, Md. R., Abdullah, U. H., Ashaari, Z., Hamid, N. H., & Hua, L. S. (2021). Hydrothermal Modification of Wood: A Review. Polymers, 13(16), 2612. https://doi.org/
10.3390/polym13162612
ASTM International. (2025). Standard Test Methods for Direct Moisture Content Measurement of Wood and Wood-Based Materials (D4442−20; Version Reapproved 2025). ASTM International. https://doi.org/10.1520/D4442-20R25
Bhuiyan, T. R., & Hirai, N. (2005). Study of crystalline behavior of heat-treated wood cellulose during treatments in water. Journal of Wood Science, 51(1), 42–47. https://doi.org/
10.1007/s10086-003-0615-x
Boonstra, M. J., & Tjeerdsma, B. (2006). Chemical analysis of heat treated softwoods. Holz Als Roh- Und Werkstoff, 64(3), 204–211. https://doi.org/10.1007/s00107-005-0078-4
Cipta, H., Kobayashi, K., Chen, S., & Sugiyama, J. (2022). Examination of Cinnamomum camphora interlocked grain adopting X-ray computed tomography combined with particle image velocimetry. Journal of Wood Science, 68(1), 56. https://doi.org/
10.1186/s10086-022-02064-z
Del Menezzi, C. H. S., Amorim, M. R. S., Costa, M. A., & Garcez, L. R. O. (2014). Evaluation of Thermally Modified Wood by Means of Stress Wave and Ultrasound Nondestructive Methods. Materials Science, 20(1), 61–66. https://doi.org/10.5755/j01.ms.20.1.3341
Esteves, B. M., & Pereira, H. M. (2009). Wood modification by heat treatment: A review. BioResources, 4(1), 370–404.
Esteves, B., Nunes, L., Lopes, R., & Cruz-Lopes, L. (2025). Enhanced Properties of Cryptomeria japonica (Thunb ex L.f.) D.Don from the Azores Through Heat-Treatment. Forests, 16(1), 166. https://doi.org/10.3390/f16010166
Garcia, R. A., De Carvalho, A. M., De Figueiredo Latorraca, J. V., De Matos, J. L. M., Santos, W. A., & De Medeiros Silva, R. F. (2012). Nondestructive evaluation of heat-treated Eucalyptus grandis Hill ex Maiden wood using stress wave method. Wood Science and Technology, 46(1–3), 41–52. https://doi.org/10.1007/s00226-010-0387-6
Hill, C. A. S. (2006). Wood Modification: Chemical, Thermal and Other Processes.
Hill, C., Altgen, M., & Rautkari, L. (2021). Thermal modification of wood—a review: Chemical changes and hygroscopicity. Journal of Materials Science, 56(11), 6581–6614. https://doi.org/10.1007/s10853-020-05722-z
Jančíková, V., & Jablonský, M. (2025). Thermal Modification of Wood—A Review. Sustainable Chemistry, 6(3), 19. https://doi.org/10.3390/suschem6030019
Laskowska, A., Kłosińska, T., & Skirko, D. (2025). Equilibrium moisture content of hydrothermally and thermo-mechanically modified oak wood. Annals of WULS, Forestry and Wood Technology, 130, 16–25. https://doi.org/10.5604/01.3001.0055.
4347
Nakagawa, T., Poulin, E., Rueppel, T., Chen, Z., Swinea, J., O’Brien, M., Houser, G., Wood, G., Weinheimer, M., Bahmani, P., Stynoski, P., & Salviato, M. (2024). Effects of thermal modification on the flexure properties, fracture energy, and hardness of western hemlock. Wood Science and Technology, 58(1), 109–133. https://doi.org/10.1007/
s00226-023-01511-4
Sun, G. R., He, Y. R., & Wu, Z. H. (2022). Effects of thermal treatment on the dimensional stability and chemical constituents of new and aged camphorwood. BioResources, 17(3), 4186–4195.
Tjeerdsma, B. F., & Militz, H. (2005). Chemical changes in hydrothermal treated wood: FTIR analysis of combined hydrothermal and dry heat-treated wood. Holz Als Roh- Und Werkstoff, 63(2), 102–111. https://doi.org/10.1007/s00107-004-0532-8
Tomak, E. D., & Ermeydan, M. A. (2025). Measuring dimensional stability of thermally modified ayous and iroko wood: Comparison of the three test methods. Cellulose, 32(4), 2581–2597. https://doi.org/10.1007/s10570-025-06404-2
Vidholdová, Z., Dudiak, M., Slabejová, G., & Výbohová, E. (2026). Hydrothermal Modification of Beech Wood. In Wood Science and Processing Engineering [Working Title]. IntechOpen. https://doi.org/10.5772/intechopen.1015232
Wang, Y., Wang, Y., Shen, L., Wu, Z., Li, H., Hu, M., Liu, Q., Chen, C., Hu, X., & Zhong, Y. (2023). Evaluation of Wood Anatomical Properties from 18 Tree Species in the Subtropical Region of China. Forests, 14(12), 2344. https://doi.org/10.3390/f14122344
Windadri, F. I., & Rahayu, S. S. B. (1999). Cinnamomum camphora (L.) J.S. Presl. In L. P. A. Oyen & X. D. Nguyen (Eds.), Plant Resources of South-East Asia No 19: Essential-oil plants. PROSEA Foundation. https://prosea.prota4u.org/view.aspx?id=655
ISSN 

